Magnetostriction.

FEATURES NIJMEGEN DRESDEN
Local Contact

Steffen WIEDMANN

Yurii Skourski

Description An optical fiber Bragg grating (FBG) method developed at the HLD is used to measure magnetostriction in pulsed magnetic fields. The relative length change ΔL/L can be obtained from the shift of the wavelength of the reflected light in the FBG [1]. (left) structure of an optical fiber Bragg grating, (right) principle of the measurement.
Field range 0 … 30 T (50 mm bore); 0 ... 38 T (32 mm bore) 0 ... 85 T. This technique can be used in all our magnets.
Temperature range 0.3 ... 4.2 K (3He system) in 50 mm bore 1.2 K … 300 K (4He system) in 50 mm bore 1.2 K … 30 K (4He system) in 32 mm bore Standard temperature range is 1.4 – 300 K. Measurements down to ~0.6 K with a 3He system are also possible.
Sample size i) in 50 mm bore < 4x4 mm2, thickness L < 3 mm ii) in 32 mm bore < 2x2 mm2, thickness L < 1.5 mm The sample size should be > 1 mm. The samples can be mounted with a defined orientation
Sensitivity Resolutions of about ΔL/L ~ 10-7 are achievable.
Typical experiments

ΔL/L(B) - magnetostriction at constant T:
Field sweep rates (typical) <0.5 … 1 T/min;
ΔL/L(T) - thermal expansion at constant B:
T sweep rates (typical) <0.5 … 1 K/min;

Magnetostriction of GdSb single crystal measured in pulsed magnetic fields [1]

Sample Holder (left) dilatometer for 50 mm bore, (middle) dilatometer for 32 mm bore, (right) dilatometer for 32 mm bore on stick.
Sample environment Gaseous helium from 270 K down to 4 K, liquid helium below
Measurement Examples The world’s smallest capacitive dilatometer: Review of Scientific Instruments 88 (2017), 083903; Field-induced states of graphite: Nature Communications 8 (2017), 1337; Lead halide perovskites: Advanced Materials 31 (2019), 1900521; Negative Thermal Expansion in frustrated spinel: Physical Review Letters 123 (2019), 027205; [1] R. Daou et al., Rev.Sci Instum. 81, 033909 (2010)
local contact: Steffen Wiedmann
local contact: Y. Skourski